Steadily {growing|expanding|developing|increasing} interest in magnetic characterization of organic compounds for therapeutic purposes or of other irregularly shaped specimens calls for refinements of experimental methodology to satisfy experimental challenges. Encapsulation in capsules remains the {method|technique|approach|strategy|system|process} of {choice|option|selection|decision}, but its applicability in precise magnetometry is {limited|restricted}. {This is|This really is|This can be|That is} {particularly|especially|specifically} {true|accurate|correct} for minute specimens {in the|within the|inside the} single milligram {range|variety} as {they are|they’re|they may be} outweighed by the capsules and are {subject|topic} to {large|big|huge|massive|substantial|significant} alignment errors. We present {here|right here} a {completely|totally|entirely|fully|absolutely} new experimental methodology that permits 30-fold in situ reduction {of the|from the|in the|on the|with the|of your} signal of capsules by substantially restoring the symmetry {of the|from the|in the|on the|with the|of your} sample holder {that is|that’s|which is|that is certainly|that is definitely|that may be} otherwise broken by the presence {of the|from the|in the|on the|with the|of your} capsule. In {practical|sensible} terms it {means|indicates|implies|signifies|suggests} that the {standard|regular|normal|common|typical} 30 mg capsule is {seen|noticed|observed} by the magnetometer as {approximately|roughly|around|about} a 1 mg object, {effectively|successfully|efficiently|properly|proficiently|correctly} opening the window for precise magnetometry of single milligram specimens. The {method|technique|approach|strategy|system|process} is shown to {work|function|perform|operate} down to 1.{8|eight} K and {in the|within the|inside the} {whole|entire|complete} {range of|selection of|array of} the magnetic fields. The {method|technique|approach|strategy|system|process} is demonstrated and validated {using|utilizing|making use of|employing|working with|applying} the reciprocal space {option|choice|alternative|selection|solution} of MPMS-SQUID magnetometers; {however|nevertheless|nonetheless|even so|on the other hand|having said that}, {it can|it could|it may|it might} be {easily|effortlessly|very easily|simply|quickly|conveniently} incorporated in any magnetometer {that can|that may|that will|that could|which will|which can} accommodate straw sample holders (i.e., the VSM-SQUID). Importantly, the {improved|enhanced} sensitivity is {accomplished|achieved} relying only {on the|around the} {standard|regular|normal|common|typical} accessories and {data|information} reduction {method|technique|approach|strategy|system|process} {provided|supplied|offered} by the SQUID manufacturer, eliminating the {need|require|want|need to have|will need|have to have} for elaborate raw {data|information} manipulations. 1250997-29-5 structure Buy55206-24-1 PMID:24733396
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