{Although|Even though|Though|Despite the fact that|While} {various|numerous|different|a variety of|several|many} spectroscopic {methods|techniques|strategies|approaches|procedures|solutions} {have been|happen to be|have already been} {developed|created} to capture the ion concentration profile {changes|modifications|adjustments|alterations}, {it is|it’s|it really is|it truly is|it can be|it is actually} {still|nonetheless|nevertheless} {difficult to|hard to|tough to} visualize the ion concentration profile and surface topographical {changes|modifications|adjustments|alterations} simultaneously {during|throughout|in the course of|for the duration of|through} the charging/discharging of LIBs. To tackle this {issue|problem|concern|situation|challenge}, {we have|we’ve|we’ve got} {developed|created} an operando scanning ion-conductance microscopy (SICM) {method|technique|approach|strategy|system|process} {that can|that may|that will|that could|which will|which can} {directly|straight} visualize an ion concentration profile and surface topography {using|utilizing|making use of|employing|working with|applying} a SICM nanopipette {whilst|while} controlling sample {potential|possible|prospective} or {current|present|existing} by potentiostat for characterizing the polarization state {during|throughout|in the course of|for the duration of|through} charging/discharging. {Using|Utilizing|Making use of|Employing|Working with|Applying} operando SICM {on the|around the} {negative|unfavorable|damaging|adverse} electrode (anode) of LIBs, {we have|we’ve|we’ve got} characterized ion concentration profile {changes|modifications|adjustments|alterations} {and the|and also the|as well as the|along with the|plus the} reversible volume {changes|modifications|adjustments|alterations} {related|associated|connected} {to the|towards the|for the} phase transition {during|throughout|in the course of|for the duration of|through} cyclic voltammetry (CV) and charge/discharge {of the|from the|in the|on the|with the|of your} {hard|difficult|tough|challenging|really hard} carbon anode. Operando SICM {is a|is really a|is actually a|can be a|is often a|is usually a} versatile {technique|method|approach|strategy} {that is|that’s|which is|that is certainly|that is definitely|that may be} {likely|most likely|probably} {to be|to become} of {major|significant|main|key|big|important} {value|worth} for evaluating correlation {of the|from the|in the|on the|with the|of your} electrolyte concentration profile and nanoscale surface topography {changes|modifications|adjustments|alterations}. 2422999-74-2 Order 37700-64-4 site PMID:23710097
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