Electrosynthetic {techniques|methods|strategies|tactics|approaches|procedures} are gaining prominenceacross the fields of chemistry, engineering and {energy|power} science. {However|Nevertheless|Nonetheless|Even so|On the other hand|Having said that}, mostworks {within|inside} the {direction|path} of synthetic heterogeneous electrocatalysis {focus|concentrate} onwater electrolysis and CO2 reduction. {In this|Within this} {work|function|perform|operate}, we moved toexpand the scope of this {technology|technologies} by {developing|creating|building|establishing} a synthetic scheme whichcouples CO2 and NH3 at a gas-liquid-solid triple-phaseboundary to {produce|create|generate|make} species with C-N bonds. {Specifically|Particularly|Especially}, by bringing in CO2from the gas phase and NH3 {from the|in the} liquid phase {together|with each other|collectively} {over|more than} solidcopper catalysts, {we have|we’ve|we’ve got} succeeded in forming formamide and acetamide productsfor {the first|the very first|the initial} time. {In a|Inside a|Within a} subsequent complementary step, {we have|we’ve|we’ve got} combinedelectrochemical {analysis|evaluation} {and a|along with a|as well as a|plus a|and also a|in addition to a} newly {developed|created} operando spectroelectrochemicalmethod, capable of probing the aforementioned triple phase boundary, to extractan initial {level of|degree of|amount of} mechanistic {analysis|evaluation} {regarding|concerning|relating to|with regards to} the reaction pathways ofthese reactions {and the|and also the|as well as the|along with the|plus the} {current|present|existing} system’s limitations. We {believe|think} that thedevelopment and understanding of this set of reaction pathways will play anexceptionally {significant|substantial|considerable|important} {role|function|part} in expanding the community’s understanding ofon-surface electrosynthetic reactions {as well|also|too|at the same time} as push this set of inherentlysustainable technologies towards widespread applicability. 159611-02-6 Chemscene BuySulfoxFluor PMID:24914310
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